I-China 75932-02-4 N-α,N-ε-di-Fmoc-D-lysine Umkhiqizi Nefekthri |Jiayinglai

75932-02-4 N-α,N-ε-di-Fmoc-D-lysine

Incazelo emfushane:

Ukubukeka	Impushana emhlophe ukuya kokumhlophe
MF	I-C36H34N2O6
MW	590.66
Ubumsulwa	98+

Thumela i-imeyili kithi

Imininingwane Yomkhiqizo

Isimo sezokuthutha&indlela yokuthumela enconyiwe:
ngomoya, ngolwandle noma nge-express

Isimo sesitoreji:
2-8°C

Ubuncane be-oda Ubuningi:
Ukuxoxisana

Isitifiketi:
I-COA, HPLC, GC, HNMR, Assay, Water Content(KF), TLC iyatholakala

Omqondofana

Na,Ne-di-Fmoc-D-lysine;

N-.ALPHA.,N-.EPSILON.-DI-FMOC-D-LYSINE;

(R)-1,13-di(9H-fluoren-9-yl)-3,11-dioxo-2,12-dioxa-4,10-diazatridecane-5-carboxylicacid;

I-D-Lysine,N2,N6-bis[(9H-fluoren-9-ylMethoxy)carbonyl]-;

I-FMoc-D-Ls(FMoc)-OHN-α,N-ε-di-FMoc-D-lysine;

N2,N6-Bis-FMoc-D-lysine;

I-N2,N6-Bis[(9H-fluoren-9-ylMethoxy)carbonyl]lysine

Ukupakisha kwangaphakathi

Ngokuvamile zisetshenziselwa ukupakisha impushana.Futhi zingavimbela ukukhanya kwelanga namanzi ukuba kungabi kubi.

ukupakisha kwangaphandle

Ibhokisi eliqinile lingavikela imikhiqizo yakho ukuthi ingaphahlazeka futhi ibe manzi.

Izinhlelo zokusebenza

Ama-amino acid avikela kabili ikakhulukazi ahlanganisa i-D-lys-OH equkethe amaqembu e-amino echungechunge oluseceleni kanye neketango eliqukethe iketangopukujikeleza kwe-L-Rag-OH.Eqenjini le-AA-amin, isu lokuvikela i-FMOC lisamukelwa, kanti umalume wesibili we-carbonate emibili usetshenziswa ochungechungeni oluseceleni.I-Tibon yethulwa eqenjini lamapayipi e-oxygenyl ukuvikela i-Fu Fu 5 ~ Sulfidal ukuze ivikele.Ngoba kunezinyathelo eziningi zokuhlanganisa zalawa ma-amino acid amabili, impendulo eyinhloko yempendulo eyinhlokosama-teps enza izivivinyo zokuthuthukisa isici esisodwa.Ukuvikelwa kwe-D-LYS-OH ikakhulukazi kubheka isikhathi esithinta isizukulwane sokulingana kwethusiiizinga lokushisa, nesikhathi sokukhumula ithusi.Ukuvikelwa kwe-L-Rag-OH ikakhulukazi kubheka ukulungiswa kwe-Z-RG-OH. Ngaleso sikhathi, izinga lokushisa le-ZL-Rag (PBF) -OH likasawoti we-ammonia, kanye nenani le-catalyst lapho i-hydrogen ihlanganiswe no-Z,

Ingcindezi, izinga lokushisa kanye nesikhathi sokusabela kuthole umphumela omuhle ngokuhlolwa kokwenza kahle.

Phakathi nenqubo yokusabela, inqubo yokusabela kokutholwa kwe-TL.C iyamukelwa ngokuyinhloko, futhi izimo zecrystallization zomkhiqizo ziyathuthukiswa.

Ukuhlanzeka komkhiqizo kukalwa nge-chromatography ye-liquid esebenza kahle kakhulu, futhi ubumsulwa bomkhiqizo bufinyelele ngaphezu kwama-95.0%.Ngaphezu kwezimpawu ezijwayelekile zomzimba ezingaguquki, futhiikuhlanganisa i-infrared spectrum, mass spectrum noma i-hydrogen spectrum.

imikhiqizo ehlobene

I-L-Ls(Boc)	Lys(Fmoc)-OH	L-Ls(Cbz)-OH	I-D-Ls(Fmoc).HCl
Lys(Fmoc).HCl	I-Boc-Ls(Boc)-OH	I-Boc-L-Ls(Boc)-OH·DCHA	I-Boc-D-Ls(Boc)-OH
I-Boc-L-Ls(Fmoc)-OH	I-Fmoc-L-Ls(tfa)-OH	I-Fmoc-L-Ls(DDC)	I-Fmoc-L-Ls(Cbz)
I-Fmoc-L-Ls(AC)	I-Fmoc-L-Ls(Fmoc)-OH	I-Fmoc-D-Ls(Boc)-OH	I-Fmoc-L-Ls(Boc)-OH
I-Cbz-L-Lys(Fmoc)-OH	Z-DL-Lys(cbz)-OH
I-Fmoc-Gly-Ol	I-Gly-Gly-Leu	I-H-Gly-Obzl.Tos	I-Boc-Trp-Gly
I-Fmoc-Gly-OH	I-Gly-Gly-Gly	I-Gly-Obzl	I-Fmoc-L-Thr(tBu)-Gly-OH
I-Fmoc-Gly-Val-OH	Ala-gly	I-Gly-Obzl.hcl	I-Met-Gly.HCl
I-Fmoc-Gly-Gly-OH	I-Ala-Gly-Ome.hcl	I-Tos-Gly-Ome	H-Met-Gly-OH
I-Fmoc-Gly-Gly-Gly-OH	I-Boc-Ala-Gly-OH	H-Gly-Oet.HCl	Cbz-D-Arg-Gly-OH
I-Fmoc-Gly-Gly-Gly-Gly-OH	I-Fmoc-Ala-gly-OH	I-Gly.HCL	I-Boc-His(Trt)-Gly-OH
H-Gly-NH2.HCl	I-Boc-Gly-OL

Ukuphakama

1. Isevisi ye-R&D iyatholakala
2. Umkhiqizi oqinisekisiwe we-ISO, isiqinisekiso sekhwalithi
I-3.Inkambo ephelele yenkonzo yokulandelela ngesikhathi sokukhiqiza
I-4.Izindleko eziphezulu
5.Imibhalo yesitifiketi sekhwalithi enikeziwe ngokwesicelo sekhasimende ngalinye
I-6.Isevisi enhle emva kokuthengisa, ukugcina ubuhlobo obuseduze nekhasimende
7.Insiza egcwele yokusiza ukwehlisa izindleko zokuthumela
8.Isampula yamahhala enikelwe ukuhlola ikhwalithi ngaphambi kwanoma iyiphi inkokhelo
9.Isikhathi sokukhokha okuxoxiswana ngaso
10.Amakhasimende e-Assit abhekana nezindaba zaseShayina